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A revolution in micronizing technology.

The Patented PulseWave Natural Resonance Disintegration technology can reduce the size of hundreds of materials to microns in less than a second without physical contact using the world’s most innovative comminution science at a fraction of the cost of standard impact mills.

com·mi·nu·tion

noun technical

/käməˈn(y)o͞oSHən/

the action of reducing a material to minute particles or fragments.

Our Science

How the PulseWave Natural Resonance Disintegration (“NRD”) Mill Works

The PulseWave NRD Mill operates on the novel principle of resonance disintegration that reduces the particle size of various materials by the application of the physics of resonance, shock waves and vortex-generated shearing forces, as opposed to the crushing and grinding processes of conventional milling methods. The design geometry of the PulseWave NRD Mill provides for a somewhat symmetrical level of the magnitude of shock waves, and the forces are phased so that the efficiency of the process is enhanced while the energy transfer to the machine is minimized. This results in materials being fragmented from within, rather than being crushed by impact or grinding which can destroy many types of materials such as high molecular weight polymers. Hence, most materials can be reduced to various particle sizes (down to colloidal size) without destroying their basic fabric or structural habit; that is, euhedral crystalline materials will tend to retain their euhedral nature when micronized by the NRD process, acicular particles will tend to retain their acicular nature, and so forth.

In addition to its ability to reduce the particle size of materials, the PulseWave NRD Mill is also capable of selective differential fragmentation of particles in complex multi-phase materials. Since different components in a heterogeneous material will have different elasticities, they will tend to resonate at differing frequencies in the NRD machine, resulting in their being separated from one another. For example, plant fiber can actually be liberated from intracellular components by the NRD process; small sections of hydraulic hose can be delaminated into separate steel wire and rubber fractions; gold particles can be liberated from sand grains; and crystalline materials are cleaved apart along the planes of their structure. Materials of heterogeneous composition are differentially fragmented with harder, less elastic components being fragmented into smaller particle sizes than softer, more elastic components. This provides the basis for "dry" fractionization. The PulseWave NRD Mill can be operated at different speeds and directions (clockwise, counterclockwise) providing versatility in particle size reduction processing.

 

Another benefit of the NRD process is that it generally produces a “tight” statistical distribution (i.e., d0.9, d0.5) of particle sizes. This results in a more uniform, consistent and predictable product. Materials can be processed in several different media including atmospheric air, water, helium or liquid nitrogen, which allows for the custom micronization of materials of various chemistry and volatility. The throughput of our standard-sized machine varies from 500 pounds to 8,000 pounds per hour, based on the size and composition of the starting material and the desired ending particle size. And finally, the PulseWave NRD process is: (a) cost effective – in most cases, materials can be reduced to a similar or smaller particle size as conventional ball or jet mills but at a fraction of the energy demand, resulting in lower processing costs and energy savings. This cost differential is particularly evident in the finer (micronic) range, often resulting in energy costs as little as one fifth or one sixth that of impact mills; and, (b) speed – material introduced into the mill is transported and processed from input to initial output in less than one second! Material reduction that takes other methods hours and days can be done in seconds and minutes in the PulseWave NRD Mill.

NRD Internal Mill Design Concept

Multiple physical forces are applied in a timed fashion to maximize the disintegrative action.

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Science

About Us

Investment Opportunities

PulseWave Holdings, Inc. (PWH) presents the patented Natural Resonance Disentigration (NRD) Mill. Our mills generate rapid pulsatile resonances, which break down both organic and inorganic materials by pulling the structures apart along natural fracture planes.  Pizoelectric effects also assist in particle disintegration.  This is quite different from simply crushing or smashing material using impact pulverization, as is the case with hammer mills, ball mills, roller mills, pin mills and other impact devices.

Our NRD mills reduce particle size (to granular or submicronic) of various materials by application of the physics of shock waves, resonance and shearing forces.  Disintegration forces are generated by addition of thousands of incremental steps.  Materials are fragmented from within rather than being crushed by impact or by grinding.  For example, crystalline materials are cleaved apart along the planes of their structure.  Materials of heterogeneous composition are differentially fragmented with harder less elastic components being fragmented into smaller particle sizes than softer, more elastic components.  This provides the basis for “dry” fractionation of materials consisting of several components.  Our machines can be operated at different speeds and directions providing versatility in particle size reduction processing.
 

Licensing Opportunities

PulseWave’s Natural Resonance Disintegration mill technology is now available for licensing. Contact us for more information about the many great advantages of licensing from PulseWave Holdings, Inc.

 

Our remarkable innovation offers significant competitive advantages:
 
  • Our standard-size NRD mill can process 500-8000 pounds per hour depending on type of material Larger and smaller design mills can be produced for specialized needs;

  • Can be operated to control heat generation to desired levels;

  • Does not destroy proteins and high molecular weight polymers;

  • Can process materials with moisture contents up to 20-30%, turning them into dry powder in the comminution process;

  • Readily fragments very hard crystalline materials;

  • Can process a wide variety of crystalline compounds and organic foodstuffs into granular or powder (micronic) consistency;

  • Provides a basis for dry fractionation of plant or other complex materials owing to diverse particle sizes that can be produced.  Hard structures fragment into smaller particles, while more elastic materials are more resilient and hence fragment into larger particles.  Example:  gold particles can be liberated from sand grains;

  • Can quickly generate stable emulsions (water-oil etc.);

  • Micronized particles can be thin-film coated with various compounds as they flow through the mill;

  • Can liberate various components from one another in the comminution process (such as silica, quartz, gold, or other minerals from an aggregate feedstock)

  • Is very energy efficient and low maintenance compared to hammer and ball mills, grinding machines, and jet mills.

About

Market Applications

Recycling

The PulseWave Natural Resonance Disintegration Milling System can micronize a variety of biomass products and waste materials to variable sizes at a fraction of the cost of conventional milling technologies while simultaneously liberating the various component parts without "smearing".

The PulseWave NRD Mill System Provides Disruptive Technology for Recycling.

1. Electrical and Electronic Equipment is the fastest growing waste stream in the world and is ideally suited for PulseWave's unique liberation technology.

2. Metals: Recyclers using aluminum and certain other metal feed stock can now reuse thousands of tons of material and save significant space in landfills using PulseWave Technology.

3. Ceramic and Porcelain tile containing natural materials such as clay, feldspar, and quartz can be micronized and returned to a powder consistency, allowing these products to be used in new manufacturing processes.

4. Biomass Materials, such as nut shells, pits and other food and food byproducts, can be micronized for a variety of useful applications.

5. Glass is 100% recyclable and can be reprocessed endlessly without loss in quality or purity - something unavailable with most food and beverage packaging options.

6. Cement Clinker, when micronized with PulseWave Technology, can be reused as a binder in cement.

These items and more offer a tremendous opportunity for recycling benefits using PulseWave's unique technology.

Food And Beverages

Micronizing food and beverage ingredients to fine particle sizes for increased yields and efficiencies provides significant advantages for varied applications.

Pharmaceuticals And Nutraceuticals

Micronization and improved oral bioavailability provide significant competitive advantages in drug and nutrient delivery.
 

The PulseWave NRD mill can be used to create liposomes that are used in the delivery of pharmaceuticals, cosmetic agents and micronutrients.  The market for liposome-formulated products is over $1 Billion and growing.

The PulseWave NRD mill can be used to create liposomes that are used in the delivery of pharmaceuticals, cosmetic agents and micronutrients.  The market for liposome-formulated products is over $1 Billion and growing.

Grains
Rice, Wheat, Corn, Barley, Soy And More

Whole grain flours are unstable without additives and special treatment. Such flours are “fortified” to overcome destabilization effects and to hold off rancidity issues for as long as possible.  If micro-fine whole seed flours can be produced that are stable (not subject to rancidity), this outcome could potentially be worth billions in nutrition industry dollars. Based on in-house research to date, it has been determined that grains processed by the PulseWave NRD Mill are sufficiently stable as to be commercially viable and free from rancidity.

Clean Coal

As part of the findings in a joint research program with the U.S. Department of Energy, Southern Illinois University (Carbondale, Illinois) and Western Research Institute (Laramie, Wyoming), PulseWave’s Natural Resonance Disintegration technology was determined to be a breakthrough technology for the efficient and cost effective comminution of coal to particle sizes suitable for pulverized coal combustion (PCC). The PulseWave NRD technology was able to show mercury reductions of 60-80% in coal that had already been processed through a conventional coal preparation plant, and further was found to reduce the inherent moisture content of Illinois coals by 60% to greater than 80% with an effective separation technology, with a concomitant ~10% increase in thermal value, without requiring additional heating of the coal. 

Oil Shale

Another joint research project in cooperation with the U.S. Department of Energy, Southern Illinois University (Carbondale, Illinois) and Western Research Institute (Laramie, Wyoming) was conducted to identify and quantify the benefits of the innovative PulseWave process that allows for the clean removal of the desirable organic material, primarily kerogen, from raw oil shale ore prior to the retorting process. Dr. John Crelling, Professor of Geology and Leader of the Maceral Separation Lab at SIU indicated that nearly 100% of the kerogen was in fact liberated from the matrix by the PulseWave process.  Dr. Crelling also found that the PulseWave process produces a “cleaner” component particle than conventional crushing techniques.  In PulseWave tests utilizing a standard kerogen concentrate and a highly purified concentrate, the oil yield for the two Fischer Assay experiments of the highly purified kerogen concentrate yielded an average of 149.1 gallons of kerogen per ton of oil shale, being a significant increase as compared with either the processed oil shale (at 32.1 gallons per ton) or the initial kerogen concentrate (60.3 gallons per ton).

Hemp

The PulseWave Natural Resonance Disintegration Mill provides a transformational technology that can instantaneously micronize complex materials while simultaneously liberating those materials one from the other without agglomeration or damage even as it reduces moisture content. The PulseWave NRD Mill has also been shown to cleanly liberate oils in grains and other materials without rupturing the natural protective sacs, and may find similar applications in hemp or other botanicals. Research and development in this field using PulseWave technology is anticipated to unlock doors for many uses of hemp and hemp biomass, including such uses as ingredients for edibles, as substitute for plastics and paper, in remediating hemp biomass for use in hempcrete or other sustainable building materials, or possibly for use in such other applications as a graphene substitute in "super batteries" or for other uses. With the myriad of possibilities for which hemp has been shown to be an effective and profitable replacement material, even as hemp biomass is rapidly escalating into a serious disposal issue, the opportunities in this field are practically endless. Research and development using the PulseWave NRD Mill may be a key to the future in this exciting field.

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As more states legalize hemp production, the opportunities for its use will continue to grow at an exponential rate.

Hemp usage in sustainable building materials is a significantly expanding market being lead by products such as hempcrete

Phosphogypsum

Phosphogypsum is a by-product of fertilizer produced from phosphate rock.  Once processed into fertilizer using acids and chemicals, the waste cannot be returned to the ground under EPA rules, since it now contains increased levels of radioactive materials. Two billion tons of this radioactive waste is currently stored in mountainous phosphogypsum stacks (better known as “gypstacks”), with 30 million new tons added each year.  These gypstacks are environmental nightmares, that can result in leeching of the hazardous chemicals into the surrounding groundwater, giant sinkholes, and many other anomalies. We believe the PulseWave NRD system can liberate the uranium, thorium and other hazards before the production stage, eliminating them from the process, thus allowing the waste products of the fertilizer production to be safely returned to the ground from whence it all came, thus eliminating those EPA-related problems while allowing for the profitable sale of the other extracted materials.

Applications
Mining (Processing Tailings)

The PulseWave Natural Resonance Disintegration (NRD) Milling System, allows the liberation of valuable metals from mining waste (tailings) as a result of its unique and proprietary technology.

The NRD milling system reduces various materials to granular, powder, or submicronic particle size by application of the physics of resonance, shock waves and shearing forces.

PulseWave's NRD mill generates rapid pulsatile resonance changes, which break down organic and inorganic materials by pulling structures apart along natural fracture planes a process which is not available in other milling technologies.

Piezoelectric effects assist in particle disintegration, which is a very different process than crushing or smashing using conventional impact pulverization such as hammer mills, ball mills, jet mills, pin mills, etc.

PulseWave's NRD mill allows unsurpassed advancements in material disintegration providing the liberation of the various components allowing recovery of high value materials.

As an example, De Beers Consolidated Mines recovered 815,036 carats of diamonds from 6,133,799 tons of tailing in 2013 and expects to continue operations beyond 2030.

DRD Gold, one of the first South African companies to abandon traditional mining to focus on extracting gold from tailings has recovered up to 40% of the gold left in particle form in tailings.  DRD Gold extracted 33,600 ounces of gold, worth nearly US$40 million, in the last quarter of 2013.

Tailings may turn out to be a viable source of another valuable and highly sought-after resource - rare earth elements.  An article appearing on ABC News, "Old Mine Tailings: New Mother Lode for Rare Elements", reported findings from the U.S. Geological Survey indicating that discarded mine tailings may yield significant amounts of rare earth elements.

Company History

PulseWave, LLC, was formed in Colorado in January 2003 to implement the research, design, development, manufacture and commercialization of a unique comminution technology.  Using experienced scientists, managers, technical and support personnel who reflected long years of qualification in new product development and manufacturing, PulseWave conducted extensive research under grants from the U.S. Department of Energy, the U.S. Department of Agriculture, the Illinois Department of Commerce and Economic Opportunity Office of Coal Development, the Illinois Clean Coal Institute, and others in conjunction with such notable institutions of higher learning as Southern Illinois University (Carbondale), Western Research Institute (Laramie, WY), University of Denver, and others  The research and testing performed by these highly specialized researchers in all relevant fields included international collaborations and project involvements with some of the world’s largest corporations.

In that process, over 150 different materials have been tested, processed, and documented using the PulseWave Natural Resonance Disintegration technology. Samples of all materials tested reside in secure company archives, with supporting records and Malvern Laser Particle Analyzer measurement graphs and results in a master computer database. A partial listing of items tested follows this section.

During this time, PulseWave had begun penetrating key markets, as its unique and proprietary NRD technology was made ready for full commercialization.

However, in about 2005, a lawsuit occurred as the result of an internal conflict that arose within the company, followed by another, and then an extended bankruptcy, all of which completely disrupted the company’s plans to move forward.

On June 29, 2016, after PulseWave had been embroiled in the bankruptcy for over ten years, Micronizing Technologies, LLC (MTL) acquired all the assets, leases, licensing rights and intellectual property of PulseWave.  Shortly thereafter, MTL began gathering all of the PulseWave assets from far and wide to its central Texas location near Dallas, began the process of reinstituting its patents, began reassembling some of the original PulseWave team members, and began re-connecting with former clients and other relevant parties.   Earlier this year, MTL established a new operating company under the name PulseWave Holdings, Inc. and is now preparing to begin full commercialization of its extraordinary PulseWave Natural Resonance Disintegration technology within the next few months
 

History
Links

Links to Grant Studies and Research

Grain

PulseWave Technology Reduces Grain to Flour at Lower Energy Costs.  Read the article from International Grain Magazine. Reference Publication #221802, Agriculture Research Service, United Stated Department of Agriculture.

Coal

PulseWave Resonance Disintegration is a breakthrough technology for the efficient and cost effective comminution of coal to fine particle sizes.  Read the Clean Coal Research Study conducted by the United States Department of Energy, Western Research Institute (Laramie, Wyoming) and Southern Illinois University, Carbondale, Illinois. 

Oil Shale

"There is no machine that is exactly like the PulseWave Resonance Disintegration Mill.  It is a novel technology and moves oil shale processing beyond the current state of the art." - quote, United States Department of Energy.  Read the full research study conducted by the United States Department of Energy, Southern Illinois University (SIU), and Western Research Institute (Laramie, Wyoming).

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Contact

Contact Us

Micronizing Technologies, LLC

Steven L. Sample, CEO
Micronizing Technologies, LLC
2806 SE 29th Street
Ocala, Florida  34471
steve.sample@pulsewavesciences.com
Tel. 352-427-6848
Fax:  (877) 513-6295

PulseWave Holdings, Inc.

Edward W. Sample, President
PulseWave Holdings, Inc.
1087 Great Meadow Drive
Allen, TX  75013

ed.sample@pulsewavesciences.com
Tel. (214) 906-3641
Fax:  (214) 317-4641

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